AB Sciex 4500 Series Manuals

AB Sciex 4500 Series Manuals

Manuals and User Guides for AB Sciex 4500 Series. We have 1 AB Sciex 4500 Series manual available for free PDF download: System User's Manual

AB Sciex 4500 Series System User's Manual

AB Sciex 4500 Series System User's Manual (142 pages)

Brand: AB Sciex | Category: Laboratory Equipment | Size: 6.47 MB

Table of Contents

Table of Contents
3
Chapter 1 Foreword

7
- General Safety Information
  7
- Symbols and Conventions
  7
- Qualified Personnel
  8
- Equipment Use and Modification
  8
- Shipping Labels
  9
- Regulatory Compliance
  9
- Australia and New Zealand
  9
- Canada
  9
- Europe
  10
- United States
  10
- International
  10
- Symbols and Labels on the Mass Spectrometer
  10
- Occupational Health and Safety Symbols
  12
- Mains Supply
  14
- Laboratory Ventilation
  14
- Environmental Conditions
  14
- Instrument Disposal (Waste Electrical and Electronic Equipment)
  15
Chapter 2 System Information

17
Chapter 3 Hardware Profiles and Projects

31
Chapter 4 Instrument Tuning and Calibrating

39
- Required Material
  39
- Prerequisites
  39
- Optimize the Instrument
  39
- Verify or Adjust Performance
  40
- Results Summary
  40
Chapter 5 Basic Acquisition Methods

43
- Create Acquisition Methods
  43
- Add an Experiment
  43
- Add a Period
  43
- Copy an Experiment into a Period
  44
- Copy an Experiment Within a Period
  44
- Scan Techniques
  44
- Quadrupole-Mode Scan Types
  44
- LIT-Mode Scan Types
  45
- About Spectral Data Acquisition
  46
- Parameters
  46
- Acquisition Method Editor Icons
  53
Chapter 6 Batches

55
- Set Queue Options
  55
- Create and Submit a Batch
  56
- Change Sample Order
  58
- Acquire Data
  58
- Set Sample Locations in the Batch Editor
  59
- Select Vial Positions Using the Locations Tab
  59
- Stop Sample Acquisition
  61
- Batch and Acquisition Method Editor Tips
  61
- Batch Editor Right-Click Menu
  62
- Queue States and Device Status
  62
- Queue States
  63
- View Instrument and Device Status Icons
  64
- Queue Right-Click Menu
  65
Chapter 7 Analyzing and Processing Data

69
- Open Data Files
  69
- Navigate between Samples in a Data File
  69
- Show Experimental Conditions
  70
- Show Data in Tables
  70
- Show ADC Data
  72
- Show Basic Quantitative Data
  72
- Chromatograms
  73
- Show Tics from a Spectrum
  73
- Show a Spectrum from a TIC
  74
- Generate Xics
  74
- Generate Bpcs
  76
- Generate Xwcs
  77
- Show DAD Data
  78
- Generate Twcs
  78
- Adjust the Threshold
  79
- Data Processing
  80
- Graphs
  81
- Zoom in on the Y-Axis
  82
- Zoom in on the X-Axis
  82
Chapter 8 Analyzing and Processing Quantitative Data

85
Appendix A Turbo V™ Ion Source User Reference

105
- Introduction to the Ion Source
  105
- Probes
  106
- Gas and Electrical Connections
  108
- Ion Source Latch
  108
- Source Exhaust System
  108
- Installation
  109
- Install the Ion Source
  109
- Optimization
  111
- Optimize the Turboionspray ® Probe
  111
- Optimize the APCI Probe
  114
- Maintenance
  116
- Clean the Probes
  116
- Remove the Ion Source
  117
- Remove the Probe
  117
- Clean the Electrode Tube
  118
- Adjust the Electrode Tip Extension
  119
- Replace the Corona Discharge Needle
  120
- Replace the Sample Tubing
  121
- Troubleshooting
  122
- Consumables
  123
Appendix B 4500 Series Instrument Requirements and Parameters

125
- Electrical and Gas Requirements
  125
- Instrument Parameters
  125
Appendix C Calibration Ions and Solutions

131
Appendix D Cleaning and Maintenance

133
- Health and Safety Precautions
  133
- Surface Cleaning
  134
- Empty the Drain Bottle
  134
- Front-End Cleaning
  135
- Best Practices
  136
- Prepare for Routine Cleaning
  137
- Clean the Curtain Plate
  138
- Clean the Front of the Orifice Plate
  139
- Put the Instrument Back into Service
  139
Appendix E Basic System Troubleshooting

141

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